Journal of Fluorine Chemistry p. 91 - 96 (1993)
Update date:2022-07-29
Topics:
Bessiere, J. M.
Boutevin, B.
El Bachiri, A.
El Harfi, A.
The synthesis of ethyl α-heptadecafluoro-undecanoyloxyacrylate (3), H2C=C(O-CO-CH2CH2C8F17)CO2CH2CH3, has been performed in three steps starting from ethyl bromopyruvate and heptadecafluoro-undecanoic acid, with an overall yield of c. 70percent.The homopolymerization and copolymerization of 3 have been easily carried out.From the kinetic study of homopolymerization and copolymerization of monomer 3 with styrene, kp2/kTe and r1, r2, the reactivity ratios of the two monomers, can be determined.
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