Journal of Organic Chemistry p. 2825 - 2828 (1983)
Update date:2022-09-26
Topics:
Barry, Carey N.
Evans, Slayton A.
The reagent triphenylphosphine-tert-butyl hypochlorite converts 1,4-diols into the corresponding tetrahydrofurans and 1,2-diols into a mixture of the regioisomeric chlorohydrins and the epoxides at -78 deg C followed by warming to ambient temperature (ca. 30 deg C).Symmetrical diols give largely chlorohydrins and dichlorides.
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