Journal of the Chemical Society, Dalton Transactions p. 993 - 994 (1984)
Update date:2022-08-02
Topics:
Davies, Stephen G.
Simpson, Stephen J.
Treatment of (Ru(η-C5H5)(PPh3)Cl) with sulphur under carbon monoxide at 1-3 atm in hot toluene gives quantitative yields of (Ru(η-C5H5)(PPh3)(CO)Cl), which can be further treated in warm methanol with CO, PMe3, and P(OPh)3 to give the cations (Ru(η-C5H5)(PPh3)(CO)2)+, (Ru(η-C5H5)(PPh3)(PMe3)(CO))+, and (Ru(η-C5H5)(PPh3)(P(OPh)3(CO))+ respectively.
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