Journal of the Chemical Society, Dalton Transactions p. 2197 - 2206 (1984)
Update date:2022-08-04
Topics:
Furlani, Anita
Licoccia, Silvia
Russo, Maria V.
Villa, Angiola Chiesi
Guastini, Carlo
Complexes cis-a water molecule forming two strong hydrogen bond with the two cis-oriented hydroxy-groups of the acetylide ligands.In all the complexes the co-ordination around platinum is distorted square planar with the acetylide ligands ?-bonded to platinum.Crystallographic details: cis-a = 15.473(5), b = 21.725(6), c = 13.439(4) Angstroem, β = 113.95(3)deg, and Z = 4; R 0.052 for 3 110 observed reflections; trans-a = 11.695(3), b = 19.690(6), c = 9.214(2) Angstroem, α = 101.88(3), β = 104.26(3), γ = 85.55(3)deg, and Z = 2; R = 0.053 for 3 961 observed reflections; a = 15.544(6), b = 12.567(4), c = 11.719(3) Angstroem, α = 91.12(3), β = 105.36(3), γ = 111.39(3)deg, and Z = 2; R = 0.046 for 4 704 observed reflections.The influence of NH3, NHEt2, and H2NNH2 on the reactivity of cis-
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