Journal of the American Chemical Society p. 2788 - 2796 (1987)
Update date:2022-08-03
Nugent, William A.
Thorn, David L.
Harlow, R. L.
The intramolecular cyclization of diacetylenes has been achieved by using either of the reagent combinations Cp2TiCl2/PMePh2/Na(Hg) or Cp2ZrCl2/Mg/HgCl2 in solvent tetrahydrofuran.The procedures are compatible with a variety of saturated functionality (O,
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