Archiv der Pharmazie p. 561 - 564 (1984)
Update date:2022-08-05
Topics:
Ruecker, Gerhard
Gajewski, Werner
Friemann, Jutta
The reaction of nardofuran (1) with alkaline hydrogen peroxide did not provide the expected epoxyketone 2, but the epoxylactone 3.Under the conditions applied this is a rare Baeyer- Villiger oxidation product.By lowering the temperature from +15 deg C to -15 deg C and by altering the molar ratio of the reactants, epoxynardofuran 2 was obtained, which is an intermediate in the formation of 3.
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