Journal of Organometallic Chemistry p. 26 - 32 (2017)
Update date:2022-08-04
Topics:
Godoy Prieto, Leonela
Lo Fiego, Marcos J.
Chopa, Alicia B.
Lockhart, María T.
A mild and mass-efficient procedure based on the one-pot diazotization-azidodediazoniation of aromatic amines is described. A wide range of aryl azides are obtained in moderate to high yields by using tributyltin azide as an effective and reusable azide source in the presence of p-toluenesulfonic acid at room temperature. The method was also successfully applied employing an insoluble polymer-supported organotin azide.
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