Nitrones by Heterolytic Fragmentation of γ-N-Hydroxyamino Sulfonates. Conversion of a Decahydroquinoline to a Perhydroazaazulene

DOI: 10.1021/jo00220a057

Source and publish data:

Journal of Organic Chemistry p. 3938 - 3940 (1985)

Update date:2022-08-05

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Authors:

LeBel, Norman A.

Caprathe, Bradley W.

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Article abstract of DOI:10.1021/jo00220a057

(E,Z)-1-Azacyclodeca-1,6-diene 1-oxide (4) was generated by fragmentation of 1-hydroxy-cis,cis-5-<(p-tolylsulfonyl)oxy>decahydroquinoline (3a) under basic conditions.The nitrone 4 underwent in situ intramolecular cycloaddition to a 1-aza-11-oxatricyclo<5.

Full text of DOI:10.1021/jo00220a057

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