Synthesis p. 427 - 431 (1994)
Update date:2022-08-04
Topics:
De Kimpe
Stanoeva
Boeykens
A convenient synthesis of monoacetals of α-diones, i.e. α-keto acetals, was developed by silver ion induced alcoholysis of regiospecifically formed α-bromo-α-chloro ketones. Similarly, the corresponding α,α-dialkoxy ketimines were synthesized from silver ion induced alcoholysis of α-bromo-α-chloro ketimines. Both methods provide an easy access to protected forms of α-diones, useful as building blocks in organic chemistry.
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Doi:10.1021/jo01355a010
(1957)Doi:10.1021/ol100645t
(2010)Doi:10.1021/jo00225a053
(1985)Doi:10.1002/jlac.198119810124
(1981)Doi:10.1016/S0040-4039(00)61960-3
(1985)Doi:10.1039/c9ra02910a
(2019)