INEPT-29Si NMR STUDY OF A TiCl4-MEDIATED REACTION OF AN ENOL SILYL ETHER

DOI: 10.1016/S0040-4039(00)98587-3

Source and publish data:

Tetrahedron Letters p. 2943 - 2946 (1985)

Update date:2022-08-03

Topics:

Authors:

Chan, T. H.

Brook, M. A.

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Article abstract of DOI:10.1016/S0040-4039(00)98587-3

Condensation of 1,3-bis(trimethylsiloxy)-1-methoxybutadiene (1) and 2-phenyl-2,2-dimethoxyethanal (2) under TiCl4 condition gave the γ-hydroxycyclopentenone product 3.The reaction was followed by INEPT-29Si NMR.Implication to the mechanism of the reaction

Full text of DOI:10.1016/S0040-4039(00)98587-3

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