Organic Process Research and Development p. 1419 - 1422 (2017)
Update date:2022-08-11
Topics:
Labes, Ricardo
Battilocchio, Claudio
Mateos, Carlos
Cumming, Graham R.
De Frutos, Oscar
Rincón, Juan A.
Binder, Kellie
Ley, Steven V.
A continuous flow method for the selective oxidation of secondary alcohols is reported. The method is based on an Oppenauer-type ruthenium-catalyzed hydrogen-transfer process that uses acetone as both solvent and oxidant. The process utilizes a low loading (1 mol%) of the commercially available ruthenium catalyst [Ru(p-cymene)Cl2]2 and triethylamine as a base and can be successfully applied to a range of different substrates, with a good level of functional group tolerance.
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