A practical and green chemical process: Fluoroalkyldistannoxane-catalyzed biphasic transesterification

DOI: 10.1002/1521-3773(20011001)40:19<3670::AID-ANIE3670>3.0.CO;2-9

Source and publish data:

Angewandte Chemie - International Edition p. 3670 - 3672 (2001)

Update date:2022-08-17

Topics:

Authors:

Xiang, Jiannan

Toyoshima, Shinji

Orita, Akihiro

Otera, Junzo

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Article abstract of DOI:10.1002/1521-3773(20011001)40:19<3670::AID-ANIE3670>3.0.CO;2-9

There is no need for the recovery of the catalyst in the fluorous biphasic transesterification catalyzed by [{Cl(C₆F₁₃CH₂CH₂)₂ SnOSn(C₆F₁₃CH₂CH₂) ₂Cl}₂] (1; see scheme), which results in quantitative conversions and yields. An FC-72 solution of the dimeric flouroalkyldistannoxane 1 can be recycled repeatedly without having to recover the neat catalyst.

Full text of DOI:10.1002/1521-3773(20011001)40:19<3670::AID-ANIE3670>3.0.CO;2-9

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