Synlett p. 279 - 280 (1997)
Update date:2022-08-11
Topics:
Jang, Doo Ok
Joo, Yung Hyup
Reaction of cyclic sulfates of vic-diols with lithium iodide in acetone produced the corresponding olefins in excellent isolated yields at low temperature. Cyclic sulfates of trans-diols gave trans-alkenes exclusively. Cyclic sulfates of cis-diols gave a mixture of cis- and trans-alkenes. The reaction offers mild conditions and easy work-up procedures.
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Doi:10.1021/ja00406a071
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