Chemical Communications p. 13798 - 13801 (2018)
Update date:2022-08-25
Topics:
Enachi, Andreea
Baabe, Dirk
Zaretzke, Marc-Kevin
Schweyen, Peter
Freytag, Matthias
Raeder, Jan
Walter, Marc D.
A novel synthesis for dialkyl cobalt compounds [(tmeda)CoR2] is presented. In these complexes tmeda is readily replaced by an NHC or a bidentate phosphine ligand to form 3- and 4-coordinate compounds, respectively. [(ItBu)Co(CH2SiMe3)2] (ItBu = 1,3-di-tert-butylimidazolin-2-ylidene) serves as an efficient, homogeneous olefin hydrogenation pre-catalyst and allows the preparation of the novel cobalt bis(alkyne) complex [(ItBu)Co(η2-PhCCPh)2].
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