Synlett p. 2959 - 2964 (2006)
Update date:2022-08-11
Topics:
Alacid, Emilio
Nájera, Carmen
A particular Kaiser oxime resin derived palladacycle is an efficient precatalyst for the Heck reaction with aryl iodides and bromides in DMF and in aqueous solvents under relatively moderate temperatures (110 °C and 120 °C) and high TON up to 105. Poisoning studies indicate that this polymer acts as a precatalyst. The polymer has been reused after recycling with low to moderate leaching of Pd(0). Georg Thieme Verlag Stuttgart.
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