Tetrahedron Letters p. 1597 - 1598 (1997)
Update date:2022-08-31
Topics:
Kim, Jae Nyoung
Jung, Keum Shin
Lee, Hong Jung
Son, Ji Suk
Isothiocyanates 2a-l were prepared in excellent yields in a one-pot reaction from aldoxime derivatives 1a-l by successive treatment of aldoxime with N-chlorosuccinimide (NCS), thiourea, and triethylamine. The use of HCl/DMF/Oxone system in the reaction instead of NCS was equally effective.
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