Russian Journal of General Chemistry p. 726 - 729 (2006)
Update date:2022-08-11
Topics:
Russavskaya
Levanova
Sukhomazova
Grabelnykh
Elaev
Klyba
Zhanchipova
Albanov
Korotaeva
Totyashinova
Korchevin
A synthesis of oligomeric substance of thiocol type, the poly(trimethyleneditelluride), from 1-bromo-3-chloropropane and elemental tellurium is performed using a hydrazine hydrate-alkali system. Reductive splitting of the tellurocol followed by alkylation with methyl iodide give rise to preparation of bis(methyltelluro)propane, which was synthesized also from dimethyltelluride and 1,3-dihalopropanes using the N2H 4?H2O/KOH system. Mass spectra of the synthesized low molecular weight organotellurium compounds are considered. Pleiades Publishing, Inc., 2006.
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