Tetrahedron Letters p. 3131 - 3134 (1982)
Update date:2022-08-16
Topics:
Nwaukwa, Stephen O.
Keehn, Philip M.
Calcium hypochlorite is an efficient reagent for the oxidation of aldehydes to the corresponding acids.Reactions are carried out at ambient temperature in aqueous acetonitrile-acetic acid solution.Aliphatic aldehydes and aromatic aldehydes with electron withdrawing groups afford good to excellent yields.Nuclear chlorination is the preferred reaction in aromatic aldehydes with electron donating groups.
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