Preparation of (5R)-5-Vinyloxazolidine-2-thione from Natural Epi-Progoitrin Using Immobilized Myrosinase

DOI: 10.1016/0957-4166(94)80145-2

Source and publish data:

Tetrahedron Asymmetry p. 1157 - 1160 (1994)

Update date:2022-08-11

Topics:

Authors:

Leoni, Onofrio

Marot, Christophe

Rollin, Patrick

Palmieri, Sandro

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Article abstract of DOI:10.1016/0957-4166(94)80145-2

Starting from (2S)-2-hydroxybut-3-enyl glucosinolate, i.e. epi-progoitrin 3, isolated from Crambe abyssinica ripe seeds, (5R)-5-vinyloxazolidine-2-thione (VOT) 8 was produced in enantiomerically pure form and high yield using a small bioreactor containing myrosinase - purified from Sinapis alba - immobilized on 18-36 mesh granular Nylon 6.6.

Full text of DOI:10.1016/0957-4166(94)80145-2

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