Journal of Organometallic Chemistry p. 99 - 112 (1994)
Update date:2022-08-17
Topics:
Herd, Oliver
Hessler, Antonella
Langhans, Klaus P.
Stelzer, Othmar
Sheldrick, William S.
Weferling, Norbert
Water soluble tertiary phosphanes 2, 7, 10-17 with sulfonated aromatic substituents p-C6H4-SO3K and 2,4-C6H3(SO3K)2 can be obtained in good yields by nucleophilic aromatic substitution of fluorine in p-F-C6H4-SO3K (1) or F-C6H3-2,4-(SO3K)2 (5) with PH3 or primary and secondary phosphanes in the superbasic medium dimethyl sulfoxide (DMSO)/KOH(solid).The first water-soluble secondary phosphane HP
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