Tetrahedron Letters p. 4141 - 4144 (1999)
Update date:2022-08-17
Topics:
Kociolek, Martin G.
Johnson, Richard P.
Flash vapor pyrolysis of 1,6,11-dodecatriyne at 500 to 600 °C and 0.01 torr affords 1,2,3,6,7,8-Hexahydro-[as]-indacene and dehydro derivatives. An uncatalyzed and highly exothermic two-step cycloaromatization mechanism is suggested. This proceeds through initial formation of a 1,4-diradical.
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