Formal synthesis of a 2- and 8-functionalized 1,4,7-trioxa-10-azaspiro[5.5]undecane

DOI: 10.1055/s-1995-3981

Source and publish data:

Synthesis p. 627 - 629 (1995)

Update date:2022-08-30

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Authors:

Lemaire Lemaire

Posada Posada

Gourcy Gourcy

Jeminet Jeminet

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Article abstract of DOI:10.1055/s-1995-3981

(E,E)-(2R,6S,8R )-(+)-N-Benzoyl-2,8-dihydroxymethyl-1,4,7-trioxa-10-azaspiro[5.5]undec ane was synthesised in seven steps from (S)-isopropylideneglycerol as chiral precursor. The final cyclodehydration reaction was carried out on a dihydroxyamidoketone intermediate.

Full text of DOI:10.1055/s-1995-3981

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