Synthesis p. 835 - 839 (1986)
Update date:2022-08-11
Topics:
Maslankiewicz, Andrzej
Skrzypek, Leszek
Chlorination of 2-, 3-, or 4-alkylthioquinolines (or -pyridines) with N-chlorosuccinimide or sulfuryl chloride affords 2-, 3-, or 4-(1-chloroalkylthio)-quinolines (or -pyridines), respetively, which in the case of ethyl or propyl compounds can be dehydrochlorinated to 1-alkenylthio derivatives. 4-Chloro-3-(1-chloroalkylthio)-quinolines react with thiourea to give 2-alkyl-1,3-dithiolo<4,5-c>quinolines.
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(2008)
