Journal of Heterocyclic Chemistry p. 779 - 781 (1995)
Update date:2022-08-11
Topics:
Mosher
Natale
Pyridinium chlorochromate oxidation of 9-methylacridine (2) affords the corresponding aldehyde 3 in good yield. Conversion of the aldehyde to the hydroximinoyl chloride 5a was accomplished via reaction of the corresponding oxime with N-chlorosuccinimide. Dipolar addition to the enamine of ethylacetoacetate provided the corresponding isoxazoles 1 in good yield.
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Doi:10.1021/ja01363a006
(1931)Doi:10.1016/0040-4039(93)88111-U
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(1996)
