Tetrahedron Letters p. 2271 - 2274 (1996)
Update date:2022-08-11
Topics:
Nishide, Kiyoharu
Shigeta, Yukihiro
Obata, Kenichi
Inoue, Takehisa
Node, Manabu
Thioethers bearing an optically active secondary alcohol were desulfurized with Raney nickel - sodium hypophosphite - acetate buffer system to give optically active alcohols without racemization in high yields. This Raney nickel combination system exhibited a unique desulfurization of benzylthio or phenylthio group in the presence of benzyl ether.
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