Journal of labelled compounds and radiopharmaceuticals p. 279 - 285 (1998)
Update date:2022-08-10
Topics:
McMorris, Trevor C.
Yu, Jian
Herman, David M.
Kelner, Michael J.
Dawe, Robin
Minamida, Akira
Tritiated derivatives of the toxic sesquiterpene illudin S (1) have been prepared by fermentation of Omphalotus illudens in the presence of [3H]- sodium acetate. [3H]-illudin S was converted to antitumor [3H]-acylfulvene (4) by treatment with dilute sulfuric acid. Antitumor [14C]- hydroxymethylacylfulvene (5) was best prepared by reacting acylfulvene with [14C]-paraformaldehyde in dilute sulfuric acid.
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