Chemistry Letters p. 223 - 224 (1996)
Update date:2022-08-11
Topics:
Shiina, Isamu
Saitoh, Masahiro
Nishimura, Koji
Saitoh, Katsuyuki
Mukaiyama, Teruaki
7β,13α-Bistriethylsiloxy-1β,2α,10β-trihydroxy -9- oxo-4(20), 11-taxadiene (2), derived from 10-deacetylbaccatin III via degradation of oxetane ring, was conveniently converted into 7-triethylsilylbaccatin III (1) by way of a new and effective method for constructing oxetane ring. Thus, the synthesis of a precursor of taxol from novel taxoid 2 was accomplished.
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