Synthesis p. 1021 - 1022 (1991)
Update date:2022-08-16
Topics:
Kudzma
Turnbull Jr.
(+)-4(5)-[1-(2,3-Dimethylphenyl)ethyl]-1H-imidazole hydrochloride (5) is prepared in three steps in 79% overall yield from 1-(N,N-dimethylsulfamoyl)imidazole by bis-protection, regioselective lithiation followed by an efficient tandem addition-reduction of the resulting 2,3-dimethylbenzoyl chloride adduct with lithium/ammonia/ammonium chloride.
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Doi:10.1016/j.ica.2019.119327
(2020)Doi:10.1016/j.catcom.2018.03.017
(2018)Doi:10.1016/j.molstruc.2020.129040
(2021)Doi:10.1021/ic300697w
(2012)Doi:10.1016/S0009-2614(97)00645-3
(1997)Doi:10.1016/j.molcata.2003.09.008
(2004)
