Organic Letters p. 764 - 767 (2016)
Update date:2022-08-11
Topics:
Patel, Niki R.
Kelly, Christopher B.
Jouffroy, Matthieu
Molander, Gary A.
Single-electron transmetalation via photoredox/nickel dual catalysis provides the opportunity for the construction of Csp3-Csp2 bonds through the transfer of alkyl radicals under very mild reaction conditions. A general procedure for the cross-coupling of primary and secondary (bis-catecholato)alkylsilicates with alkenyl halides is presented. The developed method allows not only alkenyl bromides and iodides but also previously underexplored alkenyl chlorides to be employed. (Chemical Equation Presented).
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