Journal of Fluorine Chemistry p. 433 - 435 (1990)
Update date:2022-08-16
Topics:
Folk, T. G.
Higgins, P. E.
Noftle, R. E.
N-Fluorosulfuryltrifluoroacetimide and N-chlorosulfuryltrifluoroacetimide have been prepared in high yield by a one-step reaction of trifluorothiolacetic acid with the corresponding fluoro- and chlorosulfuryl isocyanates.The trifluoroacetimides are easily purified by vacuum sublimation from the crude product mixture.
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