A Direct Preparation of Fluorinated Imides

DOI: 10.1016/S0022-1139(00)85009-5

Source and publish data:

Journal of Fluorine Chemistry p. 433 - 435 (1990)

Update date:2022-08-16

Topics:

Authors:

Folk, T. G.

Higgins, P. E.

Noftle, R. E.

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Article abstract of DOI:10.1016/S0022-1139(00)85009-5

N-Fluorosulfuryltrifluoroacetimide and N-chlorosulfuryltrifluoroacetimide have been prepared in high yield by a one-step reaction of trifluorothiolacetic acid with the corresponding fluoro- and chlorosulfuryl isocyanates.The trifluoroacetimides are easily purified by vacuum sublimation from the crude product mixture.

Full text of DOI:10.1016/S0022-1139(00)85009-5

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