Synthesis p. 757 - 758 (1992)
Update date:2022-08-11
Topics:
Kulinski
Jonczyk
Chloroacetylene (1) was synthesized as solution in hexane from 1,1-dichloroethene (2) in the presence of 50% aqueous sodium hydroxide and tetrabutylammonium hydrogen sulfate as a catalyst (PTC), in moderate yield. Reaction of 2-phenylpropiononitrile with 1 afforded the corresponding 3-butynenitrile 3 in good yield.
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Doi:10.1023/A:1011577903726
(2001)Doi:10.1016/j.tetasy.2004.05.040
(2004)Doi:10.1039/cc9960001579
(1996)Doi:10.1016/j.ica.2007.05.002
(2008)Doi:10.1016/S0008-6215(00)80495-4
(1970)Doi:10.1007/s11030-020-10117-y
(2021)
