Tetrahedron Letters p. 7607 - 7610 (1993)
Update date:2022-08-11
Topics:
Tokuda, Masao
Mimura, Nobuo
Karasawa, Tamae
Fujita, Hirotake
Suginome, Hiroshi
Reactive zinc metal can be prepared by the electrolysis of a DMF solution containing Et4NClO4 with a platinum cathode and a zinc anode. The reaction of 2-bromomethyl-1, 4-dibromo-2-butene (1) with aldehydes or ketones in the presence of the electrogenarated reactive zinc (EGZn) in DMF at 0 °C gave the corresponding isoprenylated alcohols (3a-3n) in good yields.
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