Tetrahedron p. 1759 - 1762 (1989)
Update date:2022-08-28
Topics:
Langendoen, Albert
Plug, Johannes P. M.
Koomen, Gerrit-Jan
Pandit, Upendra K.
6-Methylellipticine (6) undergoes acylation at the C(9)-position, under Friedel Crafts reaction conditions.The C(9)-formyl compound (8) rearranges to the corresponding hydroxy derivative (9) upon treatment with hydrogen peroxide, in methanol, in the presence of sulphuric acid.The two steps provide a convenient procedure for the specific C(9)-hydroxylation of the ellipticine template.
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