Bulletin of the Chemical Society of Japan p. 3690 - 3692 (1986)
Update date:2022-08-30
Topics:
Matsue, Tomokazu
Yamada, Tsukasa
Takahashi, Hiroko
Osa, Tetsuo
The electrocatalytic hydrogenation of benzylidenelactone and 5-benzylidenehydantoin with Raney-nickel proceeded smoothly to afford N-acetylphenylalanine and 5-benzylhydantoin, respectively.In addition, refluxing the electrolyte solution after the electrolysis finally yielded phenylalanine with satisfactory chemical yields and current efficiencies.This electrocatalytic process showed slightly higher reactivity than the ordinary catalytic hydrogenation.
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