Absolute stereochemistry of alloxanic acid. A configurational relay for uricase reaction

DOI: 10.1016/S0040-4039(00)60655-X

Source and publish data:

Tetrahedron Letters p. 4679 - 4682 (1993)

Update date:2022-08-11

Topics:

Authors:

Modric, Nevenka

Poje Poje

Watkin Watkin

Edwards, Alison J.

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Article abstract of DOI:10.1016/S0040-4039(00)60655-X

Alloxanic acid (3) was resolved by means of brucine and converted into its enantiomorphic esters 8 and amides 9; ethyl (-)-alloxanate whose absolute (S)-configuration was established by X-ray analysis served as configurational standard for the correlation of (+)-(R)-(3) and its precursor (-)-(S)-5-hydroxyisourate (2), the key uricolytic intermediate.

Full text of DOI:10.1016/S0040-4039(00)60655-X

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