Journal of Fluorine Chemistry p. 135 - 138 (1995)
Update date:2022-08-17
Topics:
Koroniak, Henryk
Karwatka, Piotr
Pluskota, Donata
Fiedorow, Piotr
Jankowski, Aleksander
1,3-Dimethyl-5-iodouracil reacts smoothly with perfluorovinyl- (and E/Z-pentafluoropropenyl)-zinc iodides in the presence of Pd0 as a catalyst yielding the appropriate 5-perfluoroalkenyl derivatives of uracil at high and moderate yield.In an analogous reaction, 1,3-dimethyl-6-iodouracils did not yield the expected coupling products. - Keywords: Synthesis; Perfluoroalkenyl uracils; NMR spectroscopy; Coupling products; Palladium catalyst
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