MILD AND RAPID AZIDE-MEDIATED, PALLADIUM CATALYZED CLEAVAGE OF ALLYLESTER BASED PROTECTING GROUPS

DOI: 10.1016/S0040-4039(00)73515-5

Source and publish data:

Tetrahedron Letters p. 5421 - 5424 (1994)

Update date:2022-08-16

Topics:

Authors:

Shapiro, Gideon

Buechler, Dieter

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Article abstract of DOI:10.1016/S0040-4039(00)73515-5

Under palladium catalysis various allylester protecting groups are rapidly cleaved in high yield with the reagent 8:3 trimethylsilyazide/tetrabutylammonium fluoride.The efficiency of this method mades it particularly useful for solid phase deprotections.

Full text of DOI:10.1016/S0040-4039(00)73515-5

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