Synthesis of methyl(D-glycopyranosyl azide) uronates

DOI: 10.1016/0008-6215(94)00313-5

Source and publish data:

Carbohydrate Research p. 85 - 92 (1995)

Update date:2022-08-11

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Authors:

Gyoergydeak, Zoltan

Thiem, Joachim

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Article abstract of DOI:10.1016/0008-6215(94)00313-5

Sodium hypochlorite oxidation catalysed by 2,2,6,6-tetramethylpiperidine 1-oxide (TEMPO) is shown to be a mild and efficient approach to the title uronates.In the gluco, galacto, allo, and 2-acetamido-2-deoxy-gluco series, the corresponding β- or α- and β-glycosyl azides could be smoothly oxidised and alternative preparations are compared to this access.Keywords: (D-Glycopyranosyl azide)uronates; Glycosyl azides; NaOCl-TEMPO oxidation

Full text of DOI:10.1016/0008-6215(94)00313-5

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