Journal of the Chemical Society. Perkin transactions I p. 3106 - 3110 (1981)
Update date:2022-08-28
Topics:
Capozzi, Giuseppe
Lucchini, Vittorio
Marcuzzi, Franco
Modena, Giorgio
Methyl(bismethylthio)sulphonium hexachloroantimonate (1a) reacts under mild conditions with 2-allylphenol (3a) to give 2-(methylthiomethyl)-2,3-dihydrobenzofuran (4a).Methylthiolation at position 5 in the heterocycle may also occur.With 4-substituted 2-allylphenols (3b-d) (substituents: methyl, chloro, nitro) only the corresponding 5-substituted 2-(methylthiomethyl)-2,3-dihydrobenzofurans (4b-d) are obtained.
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