Journal of the Chemical Society. Chemical communications p. 715 - 717 (1993)
Update date:2022-08-16
Topics:
Elothmani, Driss
Do, Quang Tho
Simonet, Jacques
Guillanton, Georges Le
The electrochemical oxidation of di-tert-butyl disulfide is shown to correspond to a one electron process; at 1.3 V, one carbon-sulfur bond is cleaved yielding two intermediate species; the tert-butyl cation and the radical t-BuS-S; a Ritter reaction occurs with the cation when the solvent is a nitrile and the cation dimerizes into a tetrasulfide; at a more positive potential (1.9 V) the two carbon-sulfur bonds are cleaved giving t-Bu cation and sulfur.
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