Tetrahedron Letters p. 3841 - 3844 (1985)
Update date:2022-08-17
Topics:
Shibasaki, Masakatsu
Ogawa, Yuji
Total synthesis of clavulones in naturally occurring form has been accomplished by the aldol coupling of the hydroxy-cyclopentenone 2 efficiently obtainable from 1,2-bis-trimethylsilyloxycyclopentene (4) by using 1,3-hydroxy transposition via the allylic methanesulfonate 11 and the α,β-unsaturated aldehyde 3.
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