Tetrahedron Letters p. 1767 - 1770 (1997)
Update date:2022-08-10
Topics:
Jarreton, Olivier
Skrydstrup, Troels
Beau, Jean-Marie
Mannosyl pyridylsulfones with varying C2-OH protecting groups were reacted with cyclohexanone in the presence of SmI2. With SiMe2tBu and Bn, high yields of an α-C-mannoside were obtained, In the former case no β-elimination was observed. The relative configuration of the major diastereomer obtained upon coupling with aldehydes was determined.
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