Torozova et al.
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yield of the reaction product was 0.249 g (72%), the purity de-
termined using GPC was 100%. 1H NMR (CD2Cl2, 400 MHz),
: 8.59 (d, 9 H); 8.25 (d, 6 Н); 8.02 (br.s, 3 H); 7.63—6.51
(m, 198 H). 13C NMR{1H} JMOD (CD2Cl2, 125 MHz) : 89.58
(s, Calkynyl); 89.62 (s, Calkynyl); 89.80 (s, Calkynyl); 120.70 (s, Cquat);
120.73 (s, Cquat); 121.16 (s, Cquat); 121.41 (s, CH); 121.49 (s, CH);
121.62 (s, CH); 121.81 (s, CH); 123.52 (s, Cquat); 125.40 (s, CH);
125.60 (s, CH); 126.72 (s, CH); 126.78 (s, CH); 127.08 (s, CH);
128.37 (s, CH); 128.64 (s, CH); 128.67 (s, CH); 128.76 (s, CH);
128.82 (s, CH); 129.70 (s, CH); 130.29 (s, CH); 130.31 (s, CH);
130.79 (s, CH); 131.31 (s, CH); 131.72 (s, CH); 131.81 (s, CH);
131.83 (s, CH); 131.92 (s, CH); 134.97 (s, CH); 135.18 (s, CH);
135.31 (s, CH); 135.57 (s, CH); 138.14 (s, Cquat); 138.22
(s, Cquat); 138.39 (s, Cquat); 138.56 (s, Cquat); 138.64 (s, Cquat);
138.73 (s, Cquat); 138.79 (s, Cquat); 139.79 (s, Cquat); 139.90
(s, Cquat); 139.96 (s, Cquat); 140.28 (s, Cquat); 140.42 (s, Cquat);
140.49 (s, Cquat); 140.54 (s, Cquat); 140.56 (s, Cquat); 140.87
(s, Cquat); 140.92 (s, Cquat); 140.99 (s, Cquat); 141.03 (s, Cquat);
141.19 (s, Cquat); 148.61 (s, NCH); 149.26 (s, NCH); 149.59
(s, NCH); 158.95 (s, NCC); 159.26 (s, NCC); 159.38 (s, NCC);
159.77 (s, NCC). MALDI-ToF MS, Found: m/z 4724 [М]+.
Calculated: M = 4722.
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The NMR spectra and elemental analysis were re-
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Higher Education of the Russian Federation using the
scientific equipment of the Center for the Study of
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of Organoelement Compounds of the Russian Academy
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The work was financially supported by the Russian
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Received March 25, 2019;
in revised form September 9, 2019;
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