Synthesis of (3S,4S)-4-Hydroxy-2,3,4,5-Tetrahydropyridazine-3-Carboxylic Acid, Component of Luzopeptin A.

DOI: 10.1016/0957-4166(95)00258-Q

Source and publish data:

Tetrahedron Asymmetry p. 1989 - 1994 (1995)

Update date:2022-08-16

Topics:

Authors:

Greck, Christine

Bischoff, Laurent

Genet, Jean Pierre

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Article abstract of DOI:10.1016/0957-4166(95)00258-Q

The enantioselective synthesis of (3S,4S)-4-hydroxy-2,3,4,5-tetrahydropyridazine-3-carboxylic acid 1 is described.The two stereogenic centers in anti relationship are obtained by sequential enantio and chemoselective hydrogenation of β-ketoester in presence of chiral ruthenium catalyst and diastereoselective amination of β-hydroxyester with di t-butylazodicarboxylate.

Full text of DOI:10.1016/0957-4166(95)00258-Q

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