Journal of Chemical and Engineering Data p. 119 - 123 (1986)
Update date:2022-08-30
Topics:
Koppes, William M.
Sitzmann, Michael L.
Adolph, Horst G.
The synthesis of a number of polynitroalkanediols of widely varying structure is reported.Several of the synthesis methods described constitute novel variations or improvements of known reactions: some polynitroaliphatic carboxylic acids were found to undergo the Schmidt reaction only in triflic acid as reaction medium; 3-nitropropyl acetate was advantageously prepared by a variation of the Kornblum reaction with aqueous Me2SO as solvent; 3,3-dinitropropanol was obtained by an intramolecular variant of the alkaline nitration method.
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