Tetrahedron Letters p. 465 - 466 (1980)
Update date:2022-08-28
Topics:
Jost, P.
Chaquin, P.
Kossanyi, J.
Irradiation of 2-allylcycloheptanone 3 forms a mixture of two oxetans, 4 and 5, in high yields. 11-Oxa tricyclo <5.3.11,9.0> undecane 5, which constitutes the 9/11 of the photoproducts, is decomposed thermally into a mixture of hydroazulene derivatives.Dehydrogenation of this mixture over palladium on alumina forms azulene.
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