Inorganic Chemistry p. 1076 - 1079 (1970)
Update date:2022-08-11
Topics:
Roesky, Herbert W.
Giere, Horst H.
Babb, Daniel P.
FSO2NHC(O)CFH2 was prepared by the reaction of FSO2NCO with monofluoroacetic acid with evolution of carbon dioxide. A study of the reactions of FSO2NHC(O)CFH2 and FSO2NHC(O)CF3 with PCl5 has resulted in the preparation and characterization of the compounds (Chemical Equation Presented) The reaction of FSO2N=CClCF3 with ammonia and several amines led to compounds of the general formula FSO2N=CCF3 where X = NH2, N(CH3)2, and N(C2H5)2. Partial hydrolysis of FSO2N=CClCF3 gave FSO2NHC(O)CF3. The compounds have been isolated and their structures characterized by infrared, nmr, and mass spectrometry and elemental analyses.
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Doi:10.1007/BF00576106
(1983)Doi:10.1021/jp971500q
(1997)Doi:10.1016/j.tet.2017.07.018
(2017)Doi:10.1080/00397919708004197
(1997)Doi:10.1007/BF02494520
(1998)Doi:10.1002/aoc.6211
(2021)
