Catalytic activity of various Lewis acids in the phosphorylation of primary polyfluoroalkanols with phosphoryl chloride

DOI: 10.1007/BF02494520

Source and publish data:

Russian Chemical Bulletin p. 2015 - 2016 (1998)

Update date:2022-08-11

Topics:

Authors:

Kudryavtsev

Zakharov

Kabachnik

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Article abstract of DOI:10.1007/BF02494520

The catalytic activity of SnCl₂, SnCl₄, SbCl₃, SbCl₅, and BiCl₃ in the reaction of 2,2,3,3,4,4,4-heptafluorobutanol with POCl₃ was studied. The mechanism of this reaction is discussed. Strong Lewis acids were found to be less active catalysts.

Full text of DOI:10.1007/BF02494520

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