Journal of labelled compounds and radiopharmaceuticals p. 427 - 430 (1994)
Update date:2022-08-11
Topics:
Cella
Carpenter
The preparation of 14C-labelled dimethylsilane-1,1-diol in two steps from 14C-labelled diphenyldimethylsilane is described. Aluminum chloride catalyzed protodesilylation of diphenyldimethyisilane with HCl in dichloromethane or dimethyldichlorosilane at 0-5°C affords labelled dimethyldichlorosilane which is hydrolyzed in the presence of triethylamine to afford the title compound in 45-60% yield.
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(1969)
