Tetrahedron Letters p. 1701 - 1704 (1999)
Update date:2022-08-17
Topics:
Sakurai, Yasunori
Sakaguchi, Satoshi
Ishii, Yasutaka
Carbonylation of terminal alkynes was performed using a new triple catalytic system, Pd(II)/chlorohydroquinone/NPMoV, under carbon monoxide and oxygen. For instance, phenylacetylene was converted into methyl phenylpropiolate (85%) in methanol and phenylmaleic anhydride (62%) in dioxane. The reaction did not take place in the absence of oxygen.
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